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The absorption spectra of single-component mixtures of erbium( III) chloride, holmium( III) chloride, neodymium( III) chloride, praseodymium( III) chloride, samarium( III) chloride and thulium( III) chloride were obtained in the molten salt eutectic 3LiCl–2CsCl at 723 K and were collected at various concentrations from 0 mM to approximately 200 mM (above which the solutions became saturated). Using these data and Beer's law, the molar absorptivities of the absorption bands for each lanthanide( III) chloride were obtained. More sophisticated analysis of the data was completed by building multivariate regression models based on spectra of single-component samples for each lanthanide metal studied. These models were then applied to the measurement/prediction of lanthanide( III) concentrations in a validation set comprised of complex multi-component mixtures within the molten-salt solution. The models performed well despite the complexity of the solutions/spectra.

Overall, this work presents the UV-vis Beer's law characterization of several lanthanides as well as successful application of multivariate analysis to the measurement/prediction of lanthanide concentrations in molten salts. This represents a significant improvement for materials analysis techniques, applicable for nuclear fuel pyroprocessing methods. • For reproduction of material from NJC: Reproduced from Ref.

XX with permission from the Centre National de la Recherche Scientifique (CNRS) and The Royal Society of Chemistry. • For reproduction of material from PCCP: Reproduced from Ref.

XX with permission from the PCCP Owner Societies. • For reproduction of material from PPS: Reproduced from Ref. XX with permission from the European Society for Photobiology, the European Photochemistry Association, and The Royal Society of Chemistry. • For reproduction of material from all other RSC journals and books: Reproduced from Ref. XX with permission from The Royal Society of Chemistry. If the material has been adapted instead of reproduced from the original RSC publication 'Reproduced from' can be substituted with 'Adapted from'. In all cases the Ref.

XX is the XXth reference in the list of references. If you are the author of this article you do not need to formally request permission to reproduce figures, diagrams etc. Contained in this article in third party publications or in a thesis or dissertation provided that the correct acknowledgement is given with the reproduced material. Reproduced material should be attributed as follows.